In force Publication date 04 Mar 19

Confirming the synthetic origin of perdnisolone/prednisone by GC-C-IRMS

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Project Title: Confirming the synthetic origin of perdnisolone/prednisone by GC-C-IRMS

Researchers: Prof. X. de la Torre, Prof. Botrè

Institution: Federazione Medico Sportiva Italiana, Italy

Year accepted: 2018

Summary: The aim of this study is to develop and validate a GC/C/IRMS method to confirm the origin of prednisone/prednisolone in human urine in samples collected during anti-doping sessions and showing prednisone/prednisolone concentrations between 30 and 60 ng/mL, without modifying the structure of the compounds of interest, fulfilling WADA requirements.

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